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河北天辰儀器設備有限公司


當前位置:河北天辰儀器設備有限公司>技術文章>差示掃描量熱儀有哪些常見問題及解決方法?
技術文章

差示掃描量熱儀有哪些常見問題及解決方法?

閱讀:558發(fā)布時間:2022-1-18

差示掃描量熱儀有哪些常見問題及解決方法?,差示掃描量熱儀,塑料薄膜和薄片測厚儀,土工布厚度儀,土工布CBR頂破試驗儀,土工布動態(tài)穿孔測定儀,微機控制土工合成材料拉拔儀,土工合成材料垂直滲透儀

據技術部5月18日上午09點01分透露:(/c149978/products/d.html)


YI、TCJT-30型差示掃描量熱儀概述:
TCJT-31型差示掃描量熱儀應用范圍有:對材料氧化誘導時間的測定,高分子材料的固化反應溫度和熱效應、物質相變溫度及其熱效應測定、高聚物材料的結晶、熔融溫度及其熱效應測定、高聚物材料的玻璃化轉變溫度等。實驗對象為:固態(tài)、液態(tài)、粘稠試樣,除了氣體。將試樣和參比物分別放入坩堝,置于爐中進行程序加熱,改變試樣和參比物的溫度。若參比物和試樣的熱容相同,試樣又無熱效應時,則二者的溫差近乎為“零”,此時得到條平滑的曲線。隨著溫度的增加,試樣產生了熱效應,而參比物未產生熱效應,二者之間就產生了溫差,在DTA曲線中表現為峰,溫差越大,峰也越大,溫差變化次數越多,峰的數目也越多。峰頂向上的峰稱為放熱峰,峰頂向下的峰稱為吸熱峰。
Overview of tcjt-30 differential scanning calorimeter:
Tcjt-31 differential scanning calorimeter can be used to measure the oxidation induction time of materials, the curing reaction temperature and thermal effect of polymer materials, the phase transition temperature and thermal effect of materials, the crystallization, melting temperature and thermal effect of polymer materials, and the glass transition temperature of polymer materials. The experimental objects are: solid, liquid, viscous samples, except gas. Put the sample and reference material into the crucible respectively, and then put them into the furnace for programmed heating to change the temperature of the sample and reference material. If the heat capacities of the reference material and the sample are the same, and the sample has no thermal effect, the temperature difference between them is almost "zero", and a smooth curve is obtained. With the increase of temperature, the sample has thermal effect, while the reference material has no thermal effect, there is a temperature difference between them, which shows as a peak in the DTA curve. The larger the temperature difference, the larger the peak, the more times the temperature difference changes, and the more number of peaks. The peak upward is called exothermic peak, and the peak downward is called endothermic peak.

二、TCJT-30型差示掃描量熱儀主要特點:
1、的爐體結構,更好的解析度和分辨率以及基線穩(wěn)定性;
2、數字式氣體質量流量計,控制吹掃氣體流量,數據直接記錄在數據庫中;
3、儀器可采用雙向控制(主機控制、軟件控制),界面友好,操作簡便。
The main features of tcjt-30 differential scanning calorimeter are as follows
1. New furnace structure, better resolution, resolution and baseline stability;
2. The digital gas mass flowmeter can accurately control the purge gas flow, and the data is directly recorded in the database;
3. The instrument can adopt two-way control (host control and software control), with friendly interface and easy operation.

三、TCJT-30型差示掃描量熱儀技術參數:
量程:0~±500mW
溫度范圍:室溫~800℃   風冷
升溫速率:1~80℃/min
溫度分辨率:0.1℃
溫度波動:±0.1℃
溫度重復性:±0.1℃
噪聲:0.01μW
解析度:0.01μW
度:0.1μW
靈敏度:0.1μW
控溫方式:升溫、恒溫(全程序自動控制)
曲線掃描:升溫掃描
氣氛控制:儀器自動切換
數據接口:標準USB接口
儀器標準:配有標準物質(錫),用戶可自行矯正溫度和熱焓
所有技術指標可根據用戶需求調整
 
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